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Résumé: The 21st International Congress on X-ray Optics and Microanalysis (ICXOM21) is dedicated to bring together scientists and technologists involved in fundamental and applied research in the field of micro (nano) analysis by means of X-ray beams, with emphasis on synchrotron sources, electrons and other energetic particle, or active in methodology and instrumental developments. The ICXOM21 target audience is both for people already involved in these fields, as well as newcomers. Presentations of new scientific results from scientists involved in fundamental and applied research from these fields or active in methodological and instrumental developments will be made by invited and contributing speakers, demonstrating recent progress. The conference program provides an excellent opportunity for researchers, students, scientists and technologists to share a common place for fruitful discussions, present new or state-of-art results within the conference topics, exchange information with experts already involved in these areas, as well as to establish or renew direct contacts with colleagues during the social program, poster program or at the industrial presentation.